Please use this identifier to cite or link to this item: doi:10.22028/D291-27819
Title: Ultrasonic assisted polyol-reduction of HAuCl4 for nanoparticle decoration of multiwall carbon nanotubes
Author(s): Lasserre, Federico
Suarez, Sebastian
Mücklich, Frank
Language: English
Title: Materials Research Express
Volume: 3
Issue: 12
Pages: 125007
Publisher/Platform: IOP Publishing
Year of Publication: 2016
Free key words: carbon nanotubes
gold nanoparticles
sonochemistry
polyol reduction
synthesis
DDC notations: 620 Engineering and machine engineering
Publikation type: Journal Article
Abstract: The decoration of carbon nanotubes with metallic nanoparticles has been extensively studied for different systems. Despite the fact that several routes are available for the production of these heterostructures, their complexity and large amount of different reagents severely hinder their applicability. In this study, we propose an alternative route based on an ultrasonic assisted polyol reduction, which requires lower temperatures and amount of reagents when compared to traditional methodologies. Furthermore, the used solvent (ethylene glycol) is more environmentally friendly than other common reagents, resulting in a less aggressive process. Weobserved that the proposed route provides the possibility of straightforwardly tune the final nanoparticle size by controlling simple parameters such as exposure time and relative reagent concentrations. Moreover, the influence of the bath temperature has been studied, finding an upper limit of 50 °Cfor the proposed methodology.
DOI of the first publication: 10.1088/2053-1591/3/12/125007
Link to this record: urn:nbn:de:bsz:291--ds-278194
hdl:20.500.11880/27393
http://dx.doi.org/10.22028/D291-27819
ISSN: 2053-1591
Date of registration: 11-Apr-2019
Sponsorship ID: EU-RISE Project CREATe-Network GA 644013
EU-Projectnumber: info:eu-repo/grantAgreement/EC/H2020/644013/EU//createE-Network
Faculty: NT - Naturwissenschaftlich- Technische Fakultät
Department: NT - Materialwissenschaft und Werkstofftechnik
Collections:SciDok - Der Wissenschaftsserver der Universität des Saarlandes

Files for this record:
File Description SizeFormat 
20-Lasserre et al - Ultrasonic assisted polyol-reduction_mit_Vorblatt.pdfAccepted Manuscript mit Vorblatt2,46 MBAdobe PDFView/Open


Items in SciDok are protected by copyright, with all rights reserved, unless otherwise indicated.