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Titel: Wet chemical deposition of transparent conducting coatings in glass tubes
Verfasser: Pütz, Jörg
Chalvet, F.N.
Aegerter, Michel A.
Sprache: Englisch
Erscheinungsjahr: 2003
Quelle: Thin solid films. - 442. 2003, 1/2, S. 53-59
SWD-Schlagwörter: Sol-Gel-Verfahren
Elektrische Eigenschaft
Zinn
Oxide
Tauchbeschichten
Antimon
Verdunstung
Hydrolyse
Einfachschichtpotenzial
DDC-Sachgruppe: 620 Ingenieurwissenschaften und Maschinenbau
Dokumentart : Journalartikel
Kurzfassung: A modified dip coating process was developed to deposit transparent conducting sol-gel SnO2:Sb (ATO, antimony doped tin oxide) coatings inside tubes and cavities in optical quality. The necessity for this improvement arises from the fact that the conventional dip coating process applied to tubes results in coatings with poor and non-reproducible properties, showing large variations in the thickness, an increased roughness and an island-like morphology. The main reason for this is found in a delayed and restricted solvent evaporation, due to an impediment of a laminar flow and a progressive saturation of the atmosphere inside the tube. By means of an additional exhausting pipe, a forced laminar flow was, therefore, generated inside the tube, which guarantees a fast evaporation and hydrolysis of the sol-gel films by a continuous renewal of the atmosphere. In this way, ATO coatings with an excellent thickness uniformity and a low roughness of Ra ≈ nm could be deposited on borosilicate glass tubes of 300 mm length and inner diameters down to 11 mm. After a heat treatment at temperatures up to 550 °C, single layer coatings exhibit a high optical transmission (T>85%) and a resistance down to 10 kΩ over a length of 22 cm.
Link zu diesem Datensatz: urn:nbn:de:bsz:291-scidok-25225
hdl:20.500.11880/24333
http://dx.doi.org/10.22028/D291-24277
SciDok-Publikation: 16-Dez-2009
Fakultät: Sonstige Einrichtungen
Fachrichtung: SE - INM Leibniz-Institut für Neue Materialien
Fakultät / Institution:INM
SE - Sonstige Einrichtungen

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